CAS 28578-16-7 PMK ethyl glycidate Mainly Used In Laboratory Research

CAS 28578-16-7 PMK ethyl glycidate Mainly Used In Laboratory Research

Chemical property
Methyl piperonyl epoxy-propionate is a white solid at room temperature and pressure. By means of the epoxy unit in its structure, the compound can react with a series of nucleophiles to prepare the corresponding methyl piperonyl derivatives.

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Methyl piperonyl epoxide ethyl propionate can be used as organic synthesis intermediates and pharmaceutical intermediates, mainly used in laboratory research and development process and pharmaceutical chemical production process.

CRAFT
In a dry reaction flask, the styrene precursor compound (2mmol) of methyl piperonyl ethyl epoxypropionate was dissolved in methylene chloride (20mL), and the resulting reaction solution was cooled to 0 ° C. M-chloroperoxybenzoic acid (863mg,5mmol) was slowly added to the mixture, and the resulting Chemicalbook complex was stirred at room temperature for 15 hours. After the reaction, the mixture was extracted three times with dichloromethane, all organic layers were combined, then the organic layer was washed with 5%NaHCO3 solution and salt water successively, the organic layer was dried with anhydrous sodium sulfate, and the desiccant was removed by filtration. The filtrate obtained was concentrated under vacuum to obtain the target product molecules.

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